I hope that the instruction below will serve your purpose
ds.Tables["TableName"].DefaultView.ToTable( true, "columnName"); //For Dataset (true means distinct)
OR
`ds.Tables[0].DefaultView.ToTable( true, "columnName");
// For a dataset where tableindex is 0
OR
dt.DefaultView.ToTable( true, "columnName"); //For Datatable
//Syntax is like Datatable.DefaultView.ToTable( Distinct true/false, "ColumnName");
MSDN: http://msdn.microsoft.com/en-us/library/wec2b2e6.aspx
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